Collect. Czech. Chem. Commun.
1989, 54, 1012-1018
https://doi.org/10.1135/cccc19891012
Synthesis of 4-(N-acetyl-L-tyrosyl)amino-2-iodobenzoic acid
Jiří Protivaa, Václav Křečeka, Bohumil Mácaa, Jiří Urbanb, Miloš Buděšínskýc and Miloš Procházkaa
a Department of Organic Chemistry, Charles University, 128 40 Prague 2
b Institute of Physical Chemistry and Electrochemistry, Czechoslovak Academy of Sciences, 118 40 Prague 1
c Institute of Organic Chemistry and Biochemistry, Czechoslovak Academy of Sciences, 166 10 Prague 6
Abstract
The title compound was prepared by a three-step synthesis from diacetyltyrosine (XV) and 4-amino-2-iodobenzoic acid (I). Syntheses of acid I and 4-amino-3-iodobenzoic acid (II) have been revised and modified. 1H and 13C NMR spectra of the synthesized compounds are discussed.
