Collect. Czech. Chem. Commun.
1994, 59, 1100-1104
https://doi.org/10.1135/cccc19941100
13C NMR Chemical Shift Assignments of Alkyl Chains of Histamine Analogous ω-Aminoalkylheterocycles and Bicyclic Derivatives
Martin Pohl, Wolf-Dieter Bloedorn, Clemens Mügge and Jürgen Liebscher
Fachbereich Chemie, Humboldt-Universität Berlin, Hessische Str. 1-2, D-10115 Berlin, Germany
Abstract
ω-Aminoalkylheterocycles and aromatics as well as bicyclic azolodiazepine derivatives were investigated by means of CH-COSY and INADEQUATE experiments. The 13C NMR shifts of all carbon atoms of the aminopropyl and aminobutyl moieties could be assigned. The benzylic position of the ω-aminopropyl moieties appears most upfield rather than more downfield like erroneously reported in the literature.
