Collect. Czech. Chem. Commun.
1995, 60, 224-236
https://doi.org/10.1135/cccc19950224
Acyclic Nucleoside and Nucleotide Analogs Derived from 2-Azaadenine
Dana Hocková, Milena Masojídková, Miloš Buděšínský and Antonín Holý
Institute of Organic Chemistry and Biochemistry, Academy of Sciences of the Czech Republic, 166 10 Prague 6, Czech Republic
Abstract
Alkylation of cesium salt of 2-azaadenine with appropriate synthons afforded the following acyclic analogs of nucleosides and nucleotides: (S)-9-(2,3-dihydroxypropyl)-2-azaadenine (VI), 3-(2-azaadenin-9-yl)-2-hydroxypropanoic acid (VIII), 9-(2-phosphonomethoxyethyl)-2-azaadenine (Xb), (R)-9-(2-phosphonomethoxypropyl)-2-azaadenine (XIb) and (S)-9-(3-hydroxy-2-phosphonomethoxypropyl)-2-azaadenine (XVIb). In some cases the N-2 isomers were also isolated.