Collect. Czech. Chem. Commun. 1997, 62, 761-768
https://doi.org/10.1135/cccc19970761

Silicon-29 NMR Spectra of tert-Butyldimethylsilyl and Trimethylsilyl Derivatives of Some Non-Rigid Diols

Magdalena Kvíčalováa, Vratislav Blechtaa, Krzysztof Kobylczykb, Ryszard Piekosb and Jan Schramla

a Institute of Chemical Process Fundamentals, Academy of Sciences of the Czech Republic,165 02 Prague 6-Suchdol, Czech Republic
b Department of Inorganic Chemistry, Medical University of Gdansk, 80 416 Gdansk, Poland

Individual author index pages


Other CCCC articles of these authors

  • Radim Dostál*, Michael G. S. Londesborough*, Magdalena Kvíčalová, Jan Macháček, Ivana Císařová and Zbyněk Janoušek
    Incremental iodination of the eight-vertex closo monocarborane anion [closo-1-CB7H8]–: Preparation and characterization of [closo-1-CB7H5-6,7,8-I3]– and [closo-1-CB7H2-2,3,4,6,7,8-I6]–, and the synthesis of the first eight-vertex C-methylated carborane anion [1-CH3-closo-1-CB7H4-6,7,8-I3]–
    2010, Vol. 75, Issue 9, pp. 931–947 [Abstract]
  • Ondřej Kysilka, Markéta Rybáčková, Martin Skalický, Magdalena Kvíčalová, Josef Cvačka and Jaroslav Kvíčala*
    HFPO Trimer-Based Alkyl Triflate, a Novel Building Block for Fluorous Chemistry. Preparation, Reactions and 19F gCOSY Analysis
    2008, Vol. 73, Issue 12, pp. 1799–1813 [Abstract]
  • Jan Schraml*, Jiří Hetflejš, Stanislav Šabata, Vratislav Blechta, Jan Sýkora and Jana Roithová
    Structure of Disilylated Acetoacetohydroxamic Acid
    2004, Vol. 69, Issue 7, pp. 1472–1478 [Abstract]
  • Jan Čermák*, Kateřina Auerová, Huong Thi Thu Nguyen, Vratislav Blechta, Pavel Vojtíšek and Jaroslav Kvíčala
    Synthesis of Rhodium Complexes with Novel Perfluoroalkyl Substituted Cyclopentadienyl Ligands
    2001, Vol. 66, Issue 2, pp. 382–396 [Abstract]
  • Jaroslav Podlaha, Ivana Císařová*, Ludmila Soukupová and Jan Schraml
    Molecular and Crystal Structure of Benzohydroxamic Acid and Its Ring-Substituted Derivatives
    2000, Vol. 65, Issue 8, pp. 1273–1288 [Abstract]
  • Hynek Balcar*, Jiří Čejka, Jiří Kubišta, Lidmila Petrusová, Pavel Kubát and Vratislav Blechta
    Preparation and Properties of Isomeric N-(4-Substituted Benzylidene)-4-ethynylanilines and 4-Substituted N-(4-Ethynylbenzylidene)anilines
    2000, Vol. 65, Issue 2, pp. 203–215 [Abstract]
  • Jan Čermák*, Stanislav Šabata, Vratislav Blechta and Bernard L. Shaw
    Nickel(0) and Palladium(0) Complexes with (Z,Z)-Ph2PCH2C(t-Bu)=N-N=C(t-Bu)CH2PPh2. Alkyne-to-Alkenyl Conversion in [Pd(MeOCOCCCOOMe){(Z,Z)-Ph2PCH2C(t-Bu)=N-N=C(t-Bu)CH2PPh2}]
    2000, Vol. 65, Issue 1, pp. 17–22 [Abstract]
  • Jiří Vohlídal, Jan Sedláček, Nikolay Patev, Marta Pacovská, Olivier Lavastre, Sandrine Cabioch, Pierre H. Dixneuf, Vratislav Blechta, Pavel Matějka and Hynek Balcar
    Comparative Study of Polymerization of 2-, 3- and 4-Iodophenylacetylenes with Rh-, Mo- and W-Based Catalysts
    1998, Vol. 63, Issue 11, pp. 1815–1838 [Abstract]
  • Hynek Balcar, Petr Holler, Jan Sedláček and Vratislav Blechta
    Polymerization of Nitrophenyl and 3-Diethylaminophenyl Prop-2-yn-1-yl Ethers with PdCl2. Polymers and Copolymers Characterization
    1998, Vol. 63, Issue 11, pp. 1803–1814 [Abstract]
  • Magdalena Kvíčalová, Jan Čermák, Vratislav Blechta and Jan Schraml
    Silicon-29 NMR Spectra of Trimethylsilylated Alcohols
    1997, Vol. 62, Issue 5, pp. 816–820 [Abstract]
  • Jan Čermák, Magdalena Kvíčalová and Vratislav Blechta
    Nickel(0) and Palladium(0) Complexes with 1,3,5-Triaza-7-phosphaadamantane. Catalysis of Buta-1,3-diene Oligomerization or Telomerization in an AqueousBiphasic System
    1997, Vol. 62, Issue 2, pp. 355–363 [Abstract]
  • Hynek Balcar, Jan Sedláček, Marta Pacovská and Vratislav Blechta
    Metathesis Polymerization of Phenylacetylene by Tungsten Aryloxo Complexes
    1995, Vol. 60, Issue 3, pp. 489–497 [Abstract]
  • Jan Čermák, Magdalena Kvíčalová, Jan Schraml and Martin Čapka
    Diels-Alder Self-Addition and Retroaddition of (Cyclopentadienylmethyl)triethoxysilane and Synthesis of its Permethylated Analogue
    1994, Vol. 59, Issue 2, pp. 453–456 [Abstract]
  • Jan Schraml, Vratislav Blechta and Eduard Krahé
    Long-Range 2D INADEQUATE in Structure Determination
    1992, Vol. 57, Issue 10, pp. 2005–2011 [Abstract]
  • Eva Petráková, Ivana Krupová, Jan Schraml and Ján Hirsch
    Synthesis and 13C NMR spectra of disaccharides related to glucoxylans and xyloglucans
    1991, Vol. 56, Issue 6, pp. 1300–1308 [Abstract]
  • Vratislav Blechta and Jan Schraml
    A selective INEPT experiment for the assignment of NMR lines of low-gyromagnetic ratio nuclei through long-range couplings
    1991, Vol. 56, Issue 2, pp. 258–261 [Abstract]
  • Jan Schraml, Robert Brežný, Magdalena Kvíčalová and Jan Čermák
    29Si and 13C NMR spectra of (E)-β-substituted 3-methoxy-4-trimethylsiloxystyrenes
    1990, Vol. 55, Issue 8, pp. 2038–2042 [Abstract]
  • Jan Schraml, Robert Brežný, Jan Čermák and Václav Chvalovský
    29Si and 13C NMR spectra of some substituted bis(trimethylsiloxy)benzenes
    1990, Vol. 55, Issue 8, pp. 2033–2037 [Abstract]
  • Jan Schraml, Robert Brežný and Jan Čermák
    Proximity and conformation effects in 29Si and 13C NMR spectra of di-ortho substituted trimethylsiloxybenzenes
    1990, Vol. 55, Issue 8, pp. 2027–2032 [Abstract]
  • Jan Schraml, Václav Chvalovský, Harald Jancke, Peter Koehler, Mikhail F. Larin, Vadim A. Pestunovich and Mikhail G. Voronkov
    Proximity effects in 29Si, 13C, and 1H NMR spectra of ortho substituted phenoxytrimethylsilanes
    1990, Vol. 55, Issue 8, pp. 2019–2026 [Abstract]
  • Jan Schraml and Jan Čermák
    29Si and 13C nmr spectra of trimethylsiloxy and hydroxy adamantanes reinvestigated at low concentration in deuteriochloroform solutions
    1990, Vol. 55, Issue 2, pp. 452–459 [Abstract]
  • Jan Schraml, Eva Petráková, Ján Hirsch, Raivo Teeaar and Endel Lippmaa
    Structure and 13C MAR NMR spectra of various forms of isomeric methyl xylobiosides
    1989, Vol. 54, Issue 11, pp. 3092–3101 [Abstract]
  • Jan Čermák, Vratislav Blechta and Václav Chvalovský
    Cooligomerization of propadiene with propyne catalysed by nickel(0) complexes
    1988, Vol. 53, Issue 6, pp. 1274–1286 [Abstract]
  • Jan Schraml, Eva Petráková, Ján Hirsch, Jan Čermák, Václav Chvalovský, Raivo Teeaar and Endel Lippmaa
    13C MAS NMR and 1H-29Si and 1H-13C heteronuclear correlation study of model xylooligosaccharides
    1987, Vol. 52, Issue 10, pp. 2460–2473 [Abstract]
  • Jan Schraml, Jaan Past, Jüri Puskar, Tõnis Pehk, Endel Lippmaa and Robert Brežný
    Assignment of 29Si NMR lines and determination of 29Si-13C coupling constants in pertrimethylsilylated lignin-related phenol-carboxylic acids by selective heteronuclear INADEQUATE method
    1987, Vol. 52, Issue 8, pp. 1985–1991 [Abstract]
  • Eva Petráková, Jan Schraml, Ján Hirsch, Magdalena Kvíčalová, Jan Zelený and Václav Chvalovský
    Analysis of oligosaccharides. 29Si and 13C NMR spectra of pertrimethylsilylated oligosaccharides derived from xylopyranose
    1987, Vol. 52, Issue 6, pp. 1501–1513 [Abstract]
  • Jaan Past, Jüri Puskar, Jan Schraml and Endel Lippmaa
    Assignment techniques for 29Si NMR spectra of pertrimethylsilylated products. 29Si satellites in 13C NMR spectra measured with selective 29Si decoupling
    1985, Vol. 50, Issue 9, pp. 2060–2064 [Abstract]
  • Jan Schraml, Štefan Kučár, Jan Zelený and Václav Chvalovský
    29Si (and 13C) NMR spectra of all pertrimethylsilylated O-acetyl and O-benzoyl 1,6-anhydro-β-D-glucopyranose derivatives. A test of empirical assignment rules
    1985, Vol. 50, Issue 5, pp. 1176–1183 [Abstract]
  • Jan Schraml, Michail Fedorovich Larin and Vadim Aleksandrovich Pestunovich
    Assignment techniques for 29Si NMR chemical shifts in pertrimethylsilylated products. Tests of empirical assignment rules by a modified 29Si indor
    1985, Vol. 50, Issue 2, pp. 343–347 [Abstract]
  • Jan Schraml, Aleksandr Mikhailovich Krapivin, Aleksandr Petrovich Luzin, Vladimir Mikhailovich Kilesso and Vadim Aleksandrovich Pestunovich
    29Si (and 13C) NMR spectra of modified silatranyl derivatives of some monosaccharides
    1984, Vol. 49, Issue 12, pp. 2897–2902 [Abstract]
  • Jan Schraml, Ján Hirsch, Eva Petráková, Eduard Krahé and Claus Bliefert
    Assignment of 1H and 13C NMR spectra by a combination of homo- and heteronuclear shift correlated two-dimensional NMR. Application to oligosaccharides related to arabinoxylane
    1984, Vol. 49, Issue 7, pp. 1605–1616 [Abstract]
  • Jan Schraml
    Routine use of inept technique for measurements of 29Si NMR spectra of trimethylsilyl derivatives
    1983, Vol. 48, Issue 12, pp. 3402–3406 [Abstract]
  • Jan Schraml, Micheline Grignon-dubois, Jacques Dunoguès, Harald Jancke, Günter Engelhardt and Václav Chvalovský
    NMR spectra (13C and 29Si) as a probe into the electronic structure of cyclopropylsilanes
    1983, Vol. 48, Issue 12, pp. 3396–3401 [Abstract]
  • Jan Schraml, Ján Šraga and Pavel Hrnčiar
    29Si, 13C and 1H NMR spectra of some trimethylsiloxy- and bis(trimethylsiloxy)butene isomers
    1983, Vol. 48, Issue 11, pp. 3097–3103 [Abstract]
  • Jan Schraml, Ján Šraga and Pavel Hrnčiar
    NMR spectra (29Si and 13C) of trimethylsilylated cyclic acyloins and ketones
    1983, Vol. 48, Issue 10, pp. 2937–2943 [Abstract]
  • Jan Schraml, Jaroslav Včelák, Miloslav Černý and Václav Chvalovský
    29Si NMR chemical shifts in pertrimethylsilylated 1,6-anhydro-β-D-glucopyranose derivatives. Empirical assignment from Hammett type dependence of the chemical shifts
    1983, Vol. 48, Issue 9, pp. 2503–2508 [Abstract]
  • Jan Schraml, Eva Petráková, Otomar Pihar, Ján Hirsch and Václav Chvalovský
    Pertrimethylsilylation as a method for improvement of chemical shift additivity through conformational homogenization. 1H and 13C NMR spectra of pertrimethylsilylated derivatives of methyl β-D-xylopyranosides
    1983, Vol. 48, Issue 7, pp. 1829–1841 [Abstract]
  • Eva Petráková and Jan Schraml
    13C and 1H NMR spectra of all methyl O-benzoyl-β-D-xylopyranosides. nonadditivity of acylation effects on 13C chemical shifts in deutoriochloroform solutions
    1983, Vol. 48, Issue 3, pp. 877–888 [Abstract]
  • Jan Schraml, Martin Čapka and Harald Jancke
    29Si, 13C and 31P NMR spectra of silicon-substituted ω-diphenylphosphinoalkyl silanes, (CH3)3-n(OC2H5)nSi(CH2)mP(C6H5)2
    1982, Vol. 47, Issue 3, pp. 793–801 [Abstract]
  • Seán Cawley, Jan Schraml, Petr Svoboda, Robert Ponec and Václav Chvalovský
    1H NMR spectra of some chloro-alkenes
    1981, Vol. 46, Issue 11, pp. 2924–2934 [Abstract]
  • Jan Schraml, Václav Chvalovský, Märt Mägi and Endel Lippmaa
    The role of electronic and steric effects in 29Si-NMR spectra of compounds with Si-O-C group
    1981, Vol. 46, Issue 2, pp. 377–390 [Abstract]
  • Jan Schraml, Harald Jancke, Günter Engelhardt, Luděk Vodička and Josef Hlavatý
    13C NMR spectra of hydroxy adamantanes additivity in 13C NMR spectra of dihydroxyadamantanes
    1979, Vol. 44, Issue 7, pp. 2230–2237 [Abstract]
  • Jan Schraml, Václav Chvalovský, Märt Mägi and Endel Lippmaa
    Silicon-29 and carbon-13 NMR spectra of model alkylsilanes of the type (CH3)3-nXnSi(CH2)mH
    1979, Vol. 44, Issue 3, pp. 854–865 [Abstract]
  • Jan Schraml, Václav Chvalovský, Märt Mägi and Endel Lipmaa
    Silicon-29 and carbon-13 NMR spectra of the compounds of the type (CH3)3Si(CH2)mOR
    1978, Vol. 43, Issue 12, pp. 3365–3372 [Abstract]
  • Jiří Dědina, Jan Schraml, Zdeněk Arnold and Jana Šauliová
    Homonuclear Overhauser effect study of trimethinium salts
    1978, Vol. 43, Issue 12, pp. 3356–3364 [Abstract]
  • Martin Čapka, Jan Schraml and Harold Jancke
    Synthesis and 29Si-, 13C-, and 31P-NMR spectra of (ω-diphenylphosphinoalkyl)trimethylsilanes
    1978, Vol. 43, Issue 12, pp. 3347–3355 [Abstract]
  • Jan Schraml, Nguyen-Duc Chuy, Petr Novák, Václav Chvalovský, Märt Mägi and Endel Lippmaa
    29Si, 17O, 13C, and 1H-NMR spectra of acetoxyalkylsubstituted silanes (CH3)3-nXnSi(CH2)mOC(O3)CH3
    1978, Vol. 43, Issue 12, pp. 3202–3209 [Abstract]
  • Jan Schraml, Jaroslav Včelák, Václav Chvalovský, Günter Engelhardt, Harald Jancke, Luděk Vodička and Josef Hlavatý
    29Si and 13C-NMR spectra and steric effects in mono- and bis(trimethylsiloxy)adamantanes
    1978, Vol. 43, Issue 12, pp. 3179–3191 [Abstract]
  • Věra Vaisarová, Jan Schraml and Jiří Hetflejš
    Hydrosilylation of isoprene and 2,3-dimethyl-1,3-butadiene catalysed by some nickel and palladium complexes
    1978, Vol. 43, Issue 1, pp. 265–277 [Abstract]