Collect. Czech. Chem. Commun. 2002, 67, 1035-1050
https://doi.org/10.1135/cccc20021035

Monocarbaborane Anion Chemistry. Syntheses and Structures Within the closo Nine-Vertex System

Tomáš Jelínek, Mark Thornton-Pett and John D. Kennedy*

The School of Chemistry of the University of Leeds, Leeds, LS2 9JT, U.K.

References

1. Štíbr B.: Chem. Rev. (Washington, D. C.) 1992, 92, 25. <https://doi.org/10.1021/cr00010a003>
2. Bregadze V. I.: Chem. Rev. (Washington, D. C.) 1992, 92, 209. <https://doi.org/10.1021/cr00010a002>
3. Strauss S. H.: Chem. Rev. (Washington, D. C.) 1993, 93, 927. <https://doi.org/10.1021/cr00019a005>
4. Reed C. A.: Acc. Chem. Res. 1998, 31, 133. <https://doi.org/10.1021/ar970230r>
5. Xie Z., Tsang C-W., Xue F., Mak T. C. W.: J. Organomet. Chem. 1999, 577, 197. <https://doi.org/10.1016/S0022-328X(98)01040-7>
6. Ivanov S. V., Ivanova S. M., Miller S. M., Anderson O. P., Solntsev K. A., Strauss S. H.: Inorg. Chim. Acta 1999, 289, 76. <https://doi.org/10.1016/S0020-1693(99)00060-2>
7. Peymann T., Herzog A., Knobler C. B., Hawthorne M. F.: Angew. Chem., Int. Ed. 1999, 38, 1062. <https://doi.org/10.1002/(SICI)1521-3773(19990419)38:8<1061::AID-ANIE1061>3.0.CO;2-B>
8. Morris J. H., Henderson K. W., Ol’shevskaya V. A.: J. Chem. Soc., Dalton Trans. 1998, 1951. <https://doi.org/10.1039/a800489g>
9. Douglas A. G., Janoušek Z., Kaszynski P., Young V. G.: Inorg. Chem. 1998, 37, 6361. <https://doi.org/10.1021/ic980775x>
10. See, for example: Stasko D., Reed C.A.: J. Am. Chem. Soc. 2002, 124, 1148; and references therein. <https://doi.org/10.1021/ja0118800>
11. Onak T., Drake R. P., Dunks G. B.: J. Am. Chem. Soc. 1965, 87, 2505. <https://doi.org/10.1021/ja01089a044>
12. Prince S. R., Schaeffer R.: Chem. Commun. 1968, 451.
13. Onak T., Matschei P., Groszek E.: J. Chem. Soc. A 1969, 1990. <https://doi.org/10.1039/j19690001990>
14. Knoth W. H.: J. Am. Chem. Soc. 1967, 89, 1274. <https://doi.org/10.1021/ja00981a048>
15. Knoth W. H.: Inorg. Chem. 1971, 10, 598. <https://doi.org/10.1021/ic50097a031>
16. Knoth W. H.: Inorg. Chem. 1973, 12, 785. <https://doi.org/10.1021/ic50119a010>
17. Plešek J., Jelínek T., Štíbr B., Heřmánek S.: J. Chem. Soc., Chem. Commun. 1988, 348. <https://doi.org/10.1039/c39880000348>
18. Jelínek T., Štíbr B., Plešek J., Kennedy J. D., Thornton-Pett M.: J. Chem. Soc., Dalton Trans. 1995, 431. <https://doi.org/10.1039/dt9950000431>
19a. Franken A., Kilner C. A., Thornton-Pett M., Kennedy J. D.: J. Organomet. Chem. 2002, in press, paper JOM 11359.
19b. Franken A., Ormsby D. L., Kilner C. A., Clegg W., Thornton-Pett M., Kennedy J. D.: J. Chem. Soc., Dalton Trans. 2002, 2807. <https://doi.org/10.1039/b205016c>
20a. Brellochs B.: Abstracts Tenth International Meeting on Boron Chemistry (IMEBORON X), Durham, England, July 11–16, 1999, Abstract No. CA-18, p. 82.
20b. Brellochs B. in: Contemporary Boron Chemistry (M. G. Davidson, A. K. Hughes, T. B. Marder and Wade K., Eds), p. 212. Royal Society of Chemistry, Cambridge (England) 2000.
21. Jelínek T., Štíbr B., Holub J., Bakardjiev M., Hnyk D., Ormsby D. L., Kilner C. A., Thornton-Pett M., Schanz H.-J., Wrackmeyer B., Kennedy J. D.: Chem. Commun. 2001, 1756. <https://doi.org/10.1039/b103408c>
22. Jelínek T., Kilner C. A., Thornton-Pett M., Kennedy J. D.: Chem. Commun. 2001, 1790. <https://doi.org/10.1039/b105645j>
23. Jelínek T., Štíbr B., Holub J., Bakardjiev M., Thornton-Pett M., Kennedy J. D., Tok O. L., Milius W., Wrackmeyer B.: Abstracts Second European Symposium on Boron Chemistry, EUROBORON 2, Dinard, France, September 2–7, 2001, Abstract No. P 19.
24. Fontaine X. L. R., Kennedy J. D., Thornton-Pett M., Nestor K., Štíbr B., Jelínek T., Baše K.: J. Chem. Soc., Dalton Trans. 1990, 2887. <https://doi.org/10.1039/dt9900002887>
25. Jelínek T., Kaněrová I., Holub J., Štíbr B., Tok O., Wrackmeyer B.: Manuscript in preparation, as cited in ref.21. See now also: Štíbr B., Wrackmeyer B.: J. Organomet. Chem. 2002, in press, and references therein.
26. Guggenberger J.: Inorg. Chem. 1968, 7, 2260. <https://doi.org/10.1021/ic50069a018>
27. O′Neill M. E., Wade K.: Polyhedron 1983, 2, 963. <https://doi.org/10.1016/S0277-5387(00)81417-5>
28. Jelínek T., Plešek J., Heřmánek S., Štíbr B.: Collect. Czech. Chem. Commun. 1986, 51, 819. <https://doi.org/10.1135/cccc19860819>
29. See, for example: Ivanov S. V., Rockwell J. J., Miller S. M., Anderson O. P., Solntsev K. A., Strauss S. H.: Inorg. Chem. 1996, 35, 7882; and references therein. <https://doi.org/10.1021/ic960859a>
30a. Tsang C. W., Yang Q., Tung-po Sze E., Mak T. C. W., Chan D. T. W., Xie Z.: Inorg. Chem. 2001, 39, 3582. <https://doi.org/10.1021/ic000137q>
30b. Tsang C. W., Yang Q., Tung-po Sze E., Mak T. C. W., Chan D. T. W., Xie Z.: Inorg. Chem. 2001, 39, 5851; and references therein. <https://doi.org/10.1021/ic000354r>
31. See, for example: Stasko D., Reed C. A.: J. Am. Chem. Soc. 2002, 124, 1148; and references therein. <https://doi.org/10.1021/ja0118800>
32. See, for example: Franken A., Kilner C. A., Thornton-Pett M., Kennedy J. D.: Collect. Czech. Chem. Commun. 2002, 67, 869.
33. See, for example: Kennedy J. D. in: Multinuclear NMR (J. Mason, Ed.), Chap. 8, p. 221. Plenum, New York and London 1987; and references therein.
34. Kennedy J. D., Staves J.: Z. Naturforsch. B 1979, 34, 808. <https://doi.org/10.1515/znb-1979-0610>
35a. Venable T. L., Hutton W. C., Grimes R. N.: J. Am. Chem. Soc. 1982, 104, 4716. <https://doi.org/10.1021/ja00381a053>
35b. Venable T. L., Hutton W. C., Grimes R. N.: J. Am. Chem. Soc. 1984, 106, 29. <https://doi.org/10.1021/ja00313a007>
36. Fontaine X. L. R., Kennedy J. D.: J. Chem. Soc., Chem. Commun. 1986, 779. <https://doi.org/10.1039/c39860000779>
37. Fontaine X. L. R., Kennedy J. D.: J. Chem. Soc., Dalton Trans. 1987, 1573. <https://doi.org/10.1039/dt9870001573>
38. See, for example: Beckett M. A., Bown M., Fontaine X. L. R., Greenwood N. N., Kennedy J. D., Thornton-Pett M.: J. Chem. Soc., Dalton Trans. 1988, 1969; and references therein. <https://doi.org/10.1039/dt9880001969>
39. See, for example: Ferguson G., Kennedy J. D., Fontaine X. L. R., Faridoon, Spalding T. R.: J. Chem. Soc., Dalton Trans. 1988, 2555; and references therein. <https://doi.org/10.1039/dt9880002555>
40. See, for example: Reed D.: Chem. Soc. Rev. 1993, 22, 109; and references therein. <https://doi.org/10.1039/cs9932200109>
41. See, for example: Heřmánek S.: Inorg. Chim. Acta 1999, 289, 20; and references therein. <https://doi.org/10.1016/S0020-1693(99)00055-9>
42. McFarlane W.: Proc. R. Soc. London, Ser. A 1968, 306, 185. <https://doi.org/10.1098/rspa.1968.0145>
43. Otwinowski Z., Minor W.: Methods Enzymol. 1997, 276, 307. <https://doi.org/10.1016/S0076-6879(97)76066-X>
44. COLLECT: Data Collection Strategy Program. Nonius 1999.
45. Sheldrick G. M.: Acta Crystallogr., Sect. A: Fundam. Crystallogr. 1990, 46, 467. <https://doi.org/10.1107/S0108767390000277>
46. Sheldrick G. M.: SHELX97, Program System for X-Ray Stucture Refinement. University of Göttingen, Göttingen 1997.