Collect. Czech. Chem. Commun. 2006, 71, 237-263
https://doi.org/10.1135/cccc20060237

Multistep Electrochemical Reduction Path of Clusters [Os3(CO)10(α-diimine)]: Comparison of Electrochemical and Photochemical Os-Os(α-diimine) Bond Cleavage

František Hartl* and Josephina W. M. van Outersterp

Van't Hoff Institute for Molecular Sciences, University of Amsterdam, Nieuwe Achtergracht 166, 1018 WV Amsterdam, The Netherlands

References

1a. Venäiläinen T., Pakkanen T. A., Pakkanen T. T., Iiskola E.: J. Organomet. Chem. 1986, 314, C49. <https://doi.org/10.1016/0022-328X(86)80381-3>
1b. Kiiski U., Venäiläinen T., Pakkanen T. A., Krause O.: J. Mol. Catal. 1991, 64, 163. <https://doi.org/10.1016/0304-5102(91)85108-E>
1c. Alvila L., Pakkanen T. A., Krause O.: J. Mol. Catal. 1993, 84, 145. <https://doi.org/10.1016/0304-5102(93)85047-W>
1d. Alvila L., Pursiainen J., Kiviaho J., Pakkanen T. A., Krause O.: J. Mol. Catal. 1994, 91, 335. <https://doi.org/10.1016/0304-5102(94)00044-1>
1e. Haukka M., Alvila L., Pakkanen T. A.: J. Mol. Catal. A 1995, 102, 79. <https://doi.org/10.1016/1381-1169(95)90043-8>
2. Haukka M., Venäiläinen T., Hirva P., Pakkanen T. A.: J. Organomet. Chem. 1996, 509, 163. <https://doi.org/10.1016/0022-328X(95)05826-B>
3a. Luukkanen S., Homanen P., Haukka M., Pakkanen T. A., Deronzier A., Chardon-Noblat S., Zsoldos D., Ziessel R.: Appl. Catal., A 1999, 185, 157. <https://doi.org/10.1016/S0926-860X(99)00134-9>
3b. Chardon-Noblat S., Da Costa P., Deronzier A., Haukka M., Pakkanen T. A., Ziessel R.: J. Electroanal. Chem. 2000, 490, 62. <https://doi.org/10.1016/S0022-0728(00)00228-X>
4. Masciocchi N., Sironi A., Chardon-Noblat S., Deronzier A.: Organometallics 2002, 21, 4009. <https://doi.org/10.1021/om020298x>
5. Chardon-Noblat S., Deronzier A., Ziessel R.: Collect. Czech. Chem. Commun. 2001, 66, 207; and references therein. <https://doi.org/10.1135/cccc20010207>
6. Chardon-Noblat S., Da Costa P., Deronzier A., Mahabiersing T., Hartl F.: Eur. J. Inorg. Chem. 2002, 2850. <https://doi.org/10.1002/1099-0682(200211)2002:11<2850::AID-EJIC2850>3.0.CO;2-4>
7. Hartl F., Mahabiersing T., Chardon-Noblat S., Da Costa P., Deronzier A.: Inorg. Chem. 2004, 43, 7250. <https://doi.org/10.1021/ic049216i>
8. Bruce M. I., Humphrey M. G., Snow M. R., Tiekink E. R., Wallis R. C.: J. Organomet. Chem. 1986, 314, 311. <https://doi.org/10.1016/0022-328X(86)80395-3>
9. Vergeer F. W., Calhorda M. J., Matousek P., Towrie M., Hartl F.: Dalton Trans. 2003, 4084. <https://doi.org/10.1039/b303437b>
10. van Outersterp J. W. M.: Ph.D. Thesis. University of Amsterdam, Amsterdam 1995.
11. Nijhoff J., Hartl F., van Outersterp J. W. M., Stufkens D. J., Calhorda M. J., Veiros L. F.: J. Organomet. Chem. 1999, 573, 121. <https://doi.org/10.1016/S0022-328X(98)00831-6>
12a. Bakker M. J., Hartl F., Stufkens D. J., Jina O. S., Sun X.-Z., George M. W.: Organometallics 2000, 19, 4310. <https://doi.org/10.1021/om000395v>
12b. Nijhoff J., Bakker M. J., Hartl F., Stufkens D. J., Fu W.-F., van Eldik R.: Inorg. Chem. 1998, 37, 661. <https://doi.org/10.1021/ic9707319>
12c. Nijhoff J., Hartl F., van Outersterp J. W. M., Stufkens D. J., Calhorda M. J., Veiros L. F.: J. Organomet. Chem. 1999, 573, 121. <https://doi.org/10.1016/S0022-328X(98)00831-6>
12d. van Outersterp J. W. M., Garriga Oostenbrink M. T., Nieuwenhuis H. A., Stufkens D. J., Hartl F.: Inorg. Chem. 1995, 34, 6312. <https://doi.org/10.1021/ic00129a016>
12e. Vergeer F. W., Kleverlaan C. J., Matousek P., Towrie M., Stufkens D. J., Hartl F.: Inorg. Chem. 2005, 44, 1319. <https://doi.org/10.1021/ic049191n>
13. Astruc D., Hamon M., Lacoste M., Desbois M.-H., Román E. in: Organometallic Synthesis (R. B. King, Ed.), p. 172. Elsevier, Amsterdam 1988.
14. Bossard C., Rigaut S., Astruc D., Delville M.-H., Félix G., Février-Bouvier A., Amiell J., Flandrois S., Delhaès P.: J. Chem. Soc., Chem. Commun. 1993, 333. <https://doi.org/10.1039/c39930000333>
15. Leadbeater N. E., Lewis J., Raithby P. R., Ward G. N.: J. Chem. Soc., Dalton Trans. 1999, 2511.
16. Treichel P. M., Williams J. P.: J. Organomet. Chem. 1977, 135, 39. <https://doi.org/10.1016/S0022-328X(00)91689-9>
17a. Public EPR Software Tools. National Institute of Environmental Health Sciences, available at http://epr.niehs.nih.gov/pest.html (access date September 2002).
17b. Duling D. R.: J. Magn. Reson., Ser. B 1994, 104, 105. <https://doi.org/10.1006/jmrb.1994.1062>
18. Krzystek J., Sienkiewicz A., Pardi L., Brunel L. C.: J. Magn. Reson. 1997, 125, 207. <https://doi.org/10.1006/jmre.1996.1098>
19. Gritzner G., Kůta J.: Pure Appl. Chem. 1984, 56, 461. <https://doi.org/10.1351/pac198456040461>
20. Pavlishchuk V. V., Addison A. W.: Inorg. Chim. Acta 2000, 298, 97. <https://doi.org/10.1016/S0020-1693(99)00407-7>
21a. Amatore C., Azzabi M., Calas P., Jutand A., Lefrou C., Rollin I.: J. Electroanal. Chem. 1990, 288, 45. <https://doi.org/10.1016/0022-0728(90)80024-Z>
21b. Rossenaar B. D., Hartl F., Stufkens D. J., Amatore C., Maisonhaute E., Verpeaux J.-N.: Organometallics 1997, 16, 4675. <https://doi.org/10.1021/om9702791>
22. Krejčík M., Daněk M., Hartl F.: J. Electroanal. Chem. Interfacial Electrochem. 1991, 317, 179. <https://doi.org/10.1016/0022-0728(91)85012-E>
23a. Hartl F., Luyten H., Nieuwenhuis H. A., Schoemaker G. C.: Appl. Spectrosc. 1994, 48, 1522. <https://doi.org/10.1366/0003702944027787>
23b. Mahabiersing T., Luyten H., Nieuwendam R. C., Hartl F.: Collect. Czech. Chem. Commun. 2003, 68, 1687. <https://doi.org/10.1135/cccc20031687>
24a. van Outersterp J. W. M., Hartl F., Stufkens D. J.: Inorg. Chem. 1994, 33, 2711. <https://doi.org/10.1021/ic00091a006>
24b. van Outersterp J. W. M., Hartl F., Stufkens D. J.: Organometallics 1995, 14, 3303. <https://doi.org/10.1021/om00007a034>
25. Kaim W., Kohlmann S., Lees A. J., Snoeck T. L., Stufkens D. J., Zulu M. M.: Inorg. Chim. Acta 1993, 210, 159. <https://doi.org/10.1016/S0020-1693(00)83322-8>
26. Klein A., Vogler C., Kaim W.: Organometallics 1996, 15, 236. <https://doi.org/10.1021/om950500e>
27. Kohlmann S., Kaim W.: Inorg. Chem. 1990, 29, 2909.
28. Bhattacharyya N. K., Coffy T. J., Quintana W., Salupo T. A., Bricker J. C., Shay T. B., Payne M., Shore S. G.: Organometallics 1990, 9, 2368. <https://doi.org/10.1021/om00158a038>
29. Greef R., Peat R., Peter L. M., Pletcher D., Robinson J. in: Instrumental Methods in Electrochemistry (T. J. Kemp, Ed.), Chap. 6., p. 180. Ellis Horwood Ltd., Chichester 1985.
30. Braterman P. S., Song S.-I., Kohlmann S., Vogler C., Kaim W.: J. Organomet. Chem. 1991, 411, 207. <https://doi.org/10.1016/0022-328X(91)86019-M>
31. Vergeer F. W., Lutz M., Spek A. L., Calhorda M. J., Stufkens D. J., Hartl F.: Eur. J. Inorg. Chem. 2005, 2206. <https://doi.org/10.1002/ejic.200401040>
32. Amatore C., Krusic P. J., Pedersen S. U., Verpeaux J.-N.: Organometallics 1995, 14, 640. <https://doi.org/10.1021/om00002a011>
33. Vlček A., Jr.: Coord. Chem. Rev. 2002, 208, 309; and references therein.
34a. Calhorda M. J., Hunstock E., Veiros L. F., Hartl F.: Eur. J. Inorg. Chem. 2001, 223. <https://doi.org/10.1002/1099-0682(20011)2001:1<223::AID-EJIC223>3.0.CO;2-U>
34b. Bakker M. J., Calhorda M. J., Hartl F.: Unpublished results.
35. Nijhoff J., Bakker M. A., Hartl F., Stufkens D. J.: J. Organomet. Chem. 1999, 572, 271. <https://doi.org/10.1016/S0022-328X(98)00955-3>
36. Nijhoff J., Hartl F., Stufkens D. J., Piet J. J., Warman J. M.: Chem. Commun. 1999, 991. <https://doi.org/10.1039/a902426c>
37a. Vlček A., Jr., Baumann F., Kaim W., Grevels F.-W., Hartl F.: J. Chem. Soc., Dalton Trans. 1998, 215. <https://doi.org/10.1039/a705819e>
37b. Kaim W., Kohlmann S.: Chem. Phys. Lett. 1987, 139, 365. <https://doi.org/10.1016/0009-2614(87)80574-2>
37c. Kaim W., Kohlmann S.: Inorg. Chem. 1990, 29, 2909. <https://doi.org/10.1021/ic00341a010>
37d. Kaim W., Olbrich-Deussner B., Gross R., Ernst S., Kohlmann S., Bessenbacher C. in: Importance of Paramagnetic Organometallic Radical Species in Activation, Selectivity and Catalysis (M. Chanon, Ed.), p. 283. Reidel, Dordrecht 1989.
38. Aarnts M. P., Hartl F., Peelen K., Stufkens D. J., Amatore C., Verpeaux J.-N.: Organometallics 1997, 16, 4686. <https://doi.org/10.1021/om9702800>